High Resolution Solid-State NMR of Silicate and Zeolites

High Resolution Solid-State NMR of Silicate and Zeolites
Author: Günter Engelhardt
Publisher:
Total Pages: 514
Release: 1987
Genre: Science
ISBN:

Covers the dramatic developments in the past decade in the applications of high-resolution NMR to the study of solid materials such as inorganic silicates, aluminosilicates, and in particular, zeolites. Also covers a variety of NMR methods, including conventional FT NMR techniques, used to investigate sorbate-sorbent interactions and the structure of adsorbed molecules. Gives an historical background to the subject and a concise survey of basic principles and methods of high-resolution solid-state NMR. Then covers 29Si NMR of silicate solutions; general aspects of 29Si and 27Al NMR of the silicate and aluminosilicate framework; application of 29Si and 27Al NMR to silicates, aluminosilicates, and zeolites; NMR studies of nuclei other than 29Si and 27Al in zeolites and non-zeolitic silicates; high-resolution studies of adsorbed molecules, and much more.

Solid-State NMR II

Solid-State NMR II
Author: B. Blümich
Publisher: Springer Science & Business Media
Total Pages: 220
Release: 2013-03-09
Genre: Science
ISBN: 3642500498

1. G. Engelhardt, H. Koller, Stuttgart, FRG: 29Si NMR of Inorganic Solids 2. H. Pfeifer, Leizpig, FRG: NMR of Solid Surfaces 3. A. Sebald, Bayreuth, FRG: MAS and CP/MAS NMR of Less Common Spin-1/2 Nuclei 4. C. J{ger, Mainz, FRG: Satellite Transition Spectroscopy of Quadrupolar Nuclei 5. D. Brinkmann, M. Mali, Z}rich, CH: NMR-NQR Studies of High-Temperature Superconductors.

Solid-State NMR in Zeolite Catalysis

Solid-State NMR in Zeolite Catalysis
Author: Jun Xu
Publisher: Springer
Total Pages: 267
Release: 2019-05-11
Genre: Science
ISBN: 9811369674

Solid-State NMR Characterization of Heterogeneous Catalysts and Catalytic Reactions provides a comprehensive account of state-of-the-art solid-state NMR techniques and the application of these techniques in heterogeneous catalysts and related catalytic reactions. It includes an introduction to the basic theory of solid-state NMR and various frequently used techniques. Special emphasis is placed on characterizing the framework and pore structure, active site, guest-host interaction, and synthesis mechanisms of heterogeneous catalysts using multinuclear one- and two-dimensional solid-sate NMR spectroscopy. Additionally, various in-situ solid-state NMR techniques and their applications in investigation of the mechanism of industrially important catalytic reactions are also discussed. Both the fundamentals and the latest research results are covered, making the book suitable as a reference guide for both experienced researchers in and newcomers to this field. Feng Deng is a Professor at Wuhan Institute of Physics and Mathematics, Chinese Academy of Sciences.

Zeolites and Zeolite-like Materials

Zeolites and Zeolite-like Materials
Author: Bert Sels
Publisher: Elsevier
Total Pages: 475
Release: 2016-07-29
Genre: Technology & Engineering
ISBN: 0444635149

Zeolites and Zeolite-like Materials offers a comprehensive and up-to-date review of the important areas of zeolite synthesis, characterization, and applications. Its chapters are written in an educational, easy-to-understand format for a generation of young zeolite chemists, especially those who are just starting research on the topic and need a reference that not only reflects the current state of zeolite research, but also identifies gaps and opportunities. The book demonstrates various applications of zeolites in heterogeneous catalysis and biomass conversion and identifies the endless possibilities that exist for this class of materials, their structures, functions, and future applications. In addition, it demonstrates that zeolite-like materials should be regarded as a living body developing towards new modern applications, thereby responding to the needs of modern technology challenges, including biomass conversion, medicine, laser techniques, and nanomaterial design, etc. The book will be of interest not only to zeolite-focused researchers, but also to a broad scientific and non-scientific audience. - Provides a comprehensive review of the literature pertaining to zeolites and zeolite-like materials since 2000 - Covers the chemistry of novel zeolite-like materials such as Metal-Organic Frameworks (MOFs), Covalent Organic Frameworks (COFs), hierarchical zeolite materials, new mesoporous and composite zeolite-like micro/mesoporous materials - Presents essential information of the new zeolite-like structures, with a balanced coverage of the most important areas of the zeolite research (synthesis, characterization, adsorption, catalysis, new applications of zeolites and zeolite-like materials) - Contains chapters prepared by known specialists who are members of the International Zeolite Association

High Pressure NMR

High Pressure NMR
Author: Jiri Jonas
Publisher: Springer Science & Business Media
Total Pages: 272
Release: 2012-12-06
Genre: Science
ISBN: 3642759262

In recent years, there has been a major expansion of high pressure research providing unique information about systems of interest to a wide range of scientific disciplines. Since nuclear magnetic resonance has been applied to a wide spec trum of problems in chemistry, physics and biochemistry, it is not surprising to find that high pressure NMR techniques have also had many applications in these fields of science. Clearly, the high information content of NMR experiments combined with high pressure provides a powerful tool in modern chem istry. It is the aim of this monograph, in the series on NMR Basic Principles and Progress, to illustrate the wide range of prob lems which can be successfully studied by high pressure NMR. Indeed, the various contributions in this volume discuss studies of interest to physics, chemical physics, biochemistry, and chemical reaction kinetics. In many different ways, this monograph demonstrates the power of modern experimental and theoretical techniques to investigate very complex systems. The first contribution, by D. Brinkman, deals with NMR and NQR studies of superionic conductors and high-Tc supercon ductors at high pressure. Pressure effects on phase transitions, detection of new phases, and pressure effects on diffusion and spin-lattice relaxation, represent a few of the topics discussed in this contribution of particular interest to solid state physics.

Microporous Framework Solids

Microporous Framework Solids
Author: Paul A. Wright
Publisher: Royal Society of Chemistry
Total Pages: 445
Release: 2008
Genre: Science
ISBN: 085404812X

The field of microporous solids in solid state chemistry has seen a huge expansion over the last decades with new developments in a diverse range of directions and applications. Drawing upon nature as an inspiration, scientists are continually extending known families and preparing porous solids with novel structures. In turn, the novel properties that these possess stimulate further research and applications. Microporous Framework Solids describes fundamental principles and experimental practices of the synthetic chemistry and physical characterisation of crystalline microporous solids. It al.

Verified Synthesis of Zeolitic Materials

Verified Synthesis of Zeolitic Materials
Author: H. Robson
Publisher: Gulf Professional Publishing
Total Pages: 288
Release: 2001-06-26
Genre: Architecture
ISBN: 9780444507037

Zeolite synthesis is an active field of research. As long as this continues, new phases will be discovered and new techniques for preparing existing phases will appear. This edition of Verified Synthesis of Zeolitic Materials contains all the recipes from the first edition plus 24 new recipes. Five new introductory articles have been included plus those from the first edition, some of which have been substantially revised. The XRD patterns have been recorded using different instrument settings from those in the first edition and are intended to conform to typical X-ray diffraction practice. In most cases, only the XRD pattern for the productas synthesised is printed here. The exceptions are those phases which show marked changes in the XRD pattern upon calcination.

Minerals in Soil Environments

Minerals in Soil Environments
Author: Joe Boris Dixon
Publisher: American Society of Agronomy
Total Pages: 1290
Release: 1989
Genre: Technology & Engineering
ISBN:

An introduction to soil mineralogy; Surface chemistry of soil minerals; An introduction to organic matter in mineral soils; Mineral equilibria and the soil system; Mineral occurrence in soil environments; Carboonate, halide, sulfate, and sulfide minerals; Aluminum oxides and oxyhydroxides; Iron oxides; Manganese oxides ands hydroxides; Kaolin and serpentine group minerals; The pyrophyllite-talc group; Micas; Vermiculites; Chlorites and hydroxy-interlayered vermiculite and smectite; Interstratification in layer silicates; Palygorskite and sepiolite group minerals; Zeolites in soils; Silica in soils: quartz and disordered silica polymorphs; Feldpars, olivines, pyroxenes, and amphiboles; Allophane and imogolite; Phosphate minerals; Titanium and zirconium minerals.

Annual Reports on NMR Spectroscopy

Annual Reports on NMR Spectroscopy
Author: Graham A. Webb
Publisher: Academic Press
Total Pages: 373
Release: 2012-10-05
Genre: Science
ISBN: 0123973058

Nuclear magnetic resonance (NMR) is an analytical tool used by chemists and physicists to study the structure and dynamics of molecules. In recent years, no other technique has gained such significance as NMR spectroscopy. It is used in all branches of science in which precise structural determination is required and in which the nature of interactions and reactions in solution is being studied. Annual Reports on NMR Spectroscopy has established itself as a premier means for the specialist and non-specialist alike to become familiar with new techniques and applications of NMR spectroscopy. - Annual Reports on NMR Spectroscopy has established itself as a premier means for the specialist and non-specialist alike to become familiar with new techniques and applications of NMR spectroscopy